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WOMAC pain scores were reduced by up to 4.5 points a 75.8% reduction and more than one in eight retatrutide-treated patients were completely free of knee pain at trial end

PMID: 15909815

Tryptophan oxidation is the degradation route most commonly detected by RP-HPLC in stored melanocortin analogues, with tyrosine at position 2 and histidine at position 6 secondary sites of concern, and freeze-thaw cycling accelerates both aggregation and oxidative degradation

Gradient separation was performed with water and 0.2% formic acid (Thermo Fisher Scientific, Waltham, MA, USA) as mobile phase A, and acetonitrile with 0.2% formic acid as mobile phase B