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IPA (1200 ml) was added to the obtained compound at 25-30C and stirred for 15 min at the same temperature

[0044] The cleaving in step 7) is performed with TFA:PhSMe:PhOMe:EDT:H 2 O:TIS:PhOH=8090:05:03:05:05:02:05(V:V), with TFA:PhSMe:PhOH:EDT:H 2 O=85:5:3:5:2 being preferred

Only the HMB-supplemented group achieved statistically significant decreases in both fat mass and body fat percentage, demonstrating that HMB enhanced the body composition benefits of time-restricted eating beyond what the dietary pattern alone could deliver

3 washes were performed with DMF

Cooled the mixture to 0-5 C and stirred for 60 min at the same temperature